Parameter |
Suggested Method of Analysis |
Description of Method |
Suggested Frequency |
Use of data |
pH |
EPRI Method C1 |
On-site using 2-Buffer Method calibration with pH meter |
Start and finish of each performance test run. |
Troubleshoot pH and maintain process efficiency |
Density |
EPRI Method D2 |
On-site using pre-calibrated pycnometer. |
Start and finish of each performance test run. |
Calibrate density meter and maintain process efficiency |
Slurry suspended solids content |
EPRI Method F1 |
Gravimetric |
Start and finish of each performance test run. |
Calibrate density meter and maintain process efficiency |
Carbonate |
EPRI Method N1 |
CO2 evolution, Ba(OH)2 absorption, Acid-base titration |
Start and finish of each performance test run. |
Measuere alkali loss in filter cake of mag-lime process; important for mag-lime or sodium systems. |
Alkalinity |
EPRI Method N3 |
Titrimetric |
Start and finish of each performance test run. |
Measuere alkali loss in filter cake of mag-lime process; important for mag-lime or sodium systems. |
Calcium and Magnesium |
EPRI Method J3 |
EDTA Titration |
Start and finish of each performance test run. |
To determine stoichiometry and monitor process chemistry |
Inerts |
EPRI Method J1 |
Acid Dissolution |
Start and finish of each performance test run. |
Quality indicator. Important for gypsum systems. |
Dissolved solids content (TDS) |
EPRI Method E1 |
Gravimetric |
Start and finish of each performance test run. |
Calibrate density meter for dissolved solids |
Sulfate (SO4=) |
EPRI Method L2 |
Wet chemistry methods |
Start and finish of each performance test run. |
To calculate stoichiometry and monitor process chemistry. |
Sulfite (SO3= or CaSO3.1/2H2O) |
EPRI Method M1 |
Iodometric titration |
Start and finish of each performance test run. |
To calculate stoichiometry and monitor process chemistry. |
Lime slurry particle size distribution |
EPRI Method G1 |
Wet Sieve |
Start and finish of each performance test run. |
Troubleshooting problems in milling circuit or process such as low utilization or poor gypsum quality |