Parameter |
Suggested Method of Analysis |
Description of Method |
Suggested Frequency |
Use of data |
Combined Water |
Moisture Balance |
Constant mass at 482oF (250oC) |
Start and finish of each performance test run. |
Product purity and properties |
Carbonate |
EPRI Method N1 |
CO2 evolution, Ba(OH)2absorption, Acid-base titration |
Start and finish of each performance test run. |
Measuere alkali loss in filter cake of mag-lime process; important for mag-lime or sodium systems. |
Alkalinity |
EPRI Method N3 |
Titrimetric |
Start and finish of each performance test run. |
Measuere alkali loss in filter cake of mag-lime process; important for mag-lime or sodium systems. |
Calcium and Magnesium |
EPRI Method J1 |
EDTA Titration |
Start and finish of each performance test run. |
Check for reagent quality - Product Purity. |
Sulfate (SO4=) |
EPRI Method L2 |
Wet Chemistry Method |
Start and finish of each performance test run. |
Product purity and properties |
Sulfite (SO3= or CaSO3.1/2H2O) |
EPRI Method M1 |
Iodometric titration |
Start and finish of each performance test run. |
Product purity and properties |
Inerts |
EPRI Method J1 |
Acid Dissolution |
Start and finish of each performance test run. |
Quality indicator. Important for gypsum systems. |
Solids content |
EPRI Method F1 |
Gravimetric |
Start and finish of each performance test run. |
Check density meter and indicate problems in milling circuit |
Particle size distribution |
Light Scattering Method |
Malvern |
Start and finish of each performance test run. |
Troubleshooting problems in milling circuit or process such as low utilization or poor gypsum quality |